High-yield microwave synthesis of layered Y2(OH)5NO3·xH2O materials

A. D. Yapryntsev, A. E. Baranchikov, L. S. Skogareva, A. E. Goldt, I. P. Stolyarov, O. S. Ivanova, V. V. Kozik, V. K. Ivanov

Research output: Contribution to journalArticlepeer-review

25 Citations (Scopus)

Abstract

A novel, facile, and versatile microwave-assisted method of high-yield synthesis of layered rare earth hydroxo compounds (LRHs) is proposed. Layered yttrium hydroxonitrates synthesized by the microwave-assisted technique crystallize in the form of thin hexagonal plates aggregated into spheroidal particles. Depending on the conditions of microwave-assisted hydrothermal synthesis, the formation of several phases differing in interplanar spacing along the [00l] direction is possible. The materials obtained are shown to possess good anion-exchange properties. This work provides a route to large-scale synthesis of LRH-based advanced materials. This journal is

Original languageEnglish
Pages (from-to)2667-2674
Number of pages8
JournalCrystEngComm
Volume17
Issue number13
DOIs
Publication statusPublished - 7 Apr 2015
Externally publishedYes

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